Institutional Repository of Xishuangbanna Tropical Botanical Garden
| A single-step isolation of squalene from olive oil deodorizer distillates by using centrifugal partition chromatography | |
| Xynos, Nikos; Zervos, Michail; Angelis, Apostolis; Aligiannis, Nektarios; Skaltsounis, Alexios-Leandros | |
| 2016 | |
| Source Publication | SEPARATION SCIENCE AND TECHNOLOGY
 |
| ISSN | 0149-6395 |
| Volume | 51Issue:5Pages:830-835 |
| Abstract | High added-value squalene (SQ) was purified in one step from olive oil deodorizer distillates (OODD) using preparative centrifugal partition chromatography (CPC) method, operating in the dual mode. The fractionation was performed using a non-aqueous biphasic solvent system consisting of heptane-acetonitrile-butanol (1.8:1.4:0.7, v/v/v), leading to the isolation of the target compound in 4 hours, using a preparative 1L column. Furthermore, a fast UHPLC-DAD method was developed and applied for the identification and quantification of SQ in both OODD and purified form. The content of SQ in the initial material was 23.4%, while the purity of the isolated SQ was 95.5%. The recovery of SQ was calculated at 76.3%. The productivity of the process was calculated at 234 mg/h/L. |
| Keyword | Counter-current Chromatography Extraction Components Separation Recovery Carbon Sebum |
| Subject Area | Chemistry ; Engineering |
| Indexed By | SCI |
| Document Type | 期刊论文 |
| Identifier | https://ir.xtbg.ac.cn/handle/353005/9741 |
| Collection | 文献共享 |
| Recommended Citation GB/T 7714 | Xynos, Nikos,Zervos, Michail,Angelis, Apostolis,et al. A single-step isolation of squalene from olive oil deodorizer distillates by using centrifugal partition chromatography[J]. SEPARATION SCIENCE AND TECHNOLOGY,2016,51(5):830-835. |
| APA | Xynos, Nikos,Zervos, Michail,Angelis, Apostolis,Aligiannis, Nektarios,&Skaltsounis, Alexios-Leandros.(2016).A single-step isolation of squalene from olive oil deodorizer distillates by using centrifugal partition chromatography.SEPARATION SCIENCE AND TECHNOLOGY,51(5),830-835. |
| MLA | Xynos, Nikos,et al."A single-step isolation of squalene from olive oil deodorizer distillates by using centrifugal partition chromatography".SEPARATION SCIENCE AND TECHNOLOGY 51.5(2016):830-835. |
| Files in This Item: | Download All | |||||
| File Name/Size | DocType | Version | Access | License | ||
| A single-step isolat（572KB） | 开放获取 | CC BY-NC-SA | View Download | |||
Items in the repository are protected by copyright, with all rights reserved, unless otherwise indicated.
Edit Comment